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全部话题 - 话题: cd2cl2
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m****g
发帖数: 988
1
PtCl2在CD2Cl2里的溶解度实在太低,做个核磁恐怕是做不出来东东,有谁碰巧知道这
个chemical shift的吗?
非常感谢!
a*****c
发帖数: 3525
2
来自主题: Macromolecules版 - How to identify this polymer
IR,left:3100-3000 cm-1 C-H (aromatic); 1600-1400 cm-1 C=C (aromatic)
right:3200-3600 cm-1 O-H; 2960-2850 cm-1, C-H (alkyl)
UV-vis, left: observable about 200-400 nm region;
right: almost none
1NMR, left: solvent: CDCl3/CD2Cl2/etc. ~7-8ppm, protons of phenyl ring,
~2-4ppm, of protons of the main chain.
right: solvent: D2O/CD3COCD3/(CD3)2SO/etc. proton of OH, and protons of
the main chain are different.
MS, fragments are different
elemental analysis, C, H.
and more if necessary.
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