c*****n 发帖数: 195 | 1 最近要从同位素标记的Histidine合成Fmoc-His(Trt)-OH, 产物买不到,查了一下
Scifinder居然没有很高效的相关合成方法,有过类似经验的能否提供一下工业上大量
制成的有效方法?原料很贵,失误不起。谢过了 | O*C 发帖数: 649 | 2 Our group use this for radio assay a lot, I don't think they ever have any
problem for labeling it, they used iodine, if I am not wrong. And they are
biologist, I think they have an protocol to label it. | c*****n 发帖数: 195 | 3 谢谢,可能是我描述的有些误差,我是买到13C labeled Histidine (no protection
group), 现在想加上Fmoc 和Trt两个保护基,如果哪位有相关经验? | t*******e 发帖数: 440 | |
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